УДК: 54.057

Synthesis and study of nanocrystalline powders for an optical ceramic composed of magnesium aluminate spinel

Tolstikova, D.V., Golieva, E.V., Lebanin, V.S., Mikhailov, M.D., Dunaev, A.A., Vetrov, V.N., Ignatenkov, B.A.

Publication in Journal of Optical Technology

For Russian citation (Opticheskii Zhurnal):

Толстикова Д.В., Гольева Е.В., Лебанин В.С., Михайлов М.Д., Дунаев А.А., Ветров В.Н., Игнатенков Б.А. Синтез и исследование нанокристаллических порошков для оптической керамики из алюмомагниевой шпинели // Оптический журнал. 2014. Т. 81. № 12. С. 69–73.

Tolstikova D.V., Golieva E.V., Lebanin V.S., Mikhailov M.D., Dunaev A.A., Vetrov V.N., Ignatenkov B.A. Synthesis and study of nanocrystalline powders for an optical ceramic composed of magnesium aluminate spinel [in Russian] // Opticheskii Zhurnal. 2014. V. 81. № 12. P. 69–73.

For citation (Journal of Optical Technology):

D. V. Tolstikova, E. V. Gol’eva, V. S. Lebanin, M. D. Mikhaĭlov, A. A. Dunaev, V. N. Vetrov, and B. A. Ignatenkov, "Synthesis and study of nanocrystalline powders for an optical ceramic composed of magnesium aluminate spinel," Journal of Optical Technology. 81(12), 754-757 (2014). https://doi.org/10.1364/JOT.81.000754

Abstract:

Nanocrystalline powders of magnesium aluminate spinel (MgAl2O4) have been produced, and their morphological and structural properties have been studied. A comparative analysis of spinel samples synthesized by different liquid-phase methods has been carried out. Hot uniaxial pressing has been used to fabricate ceramic samples of spinel 15 mm in diameter and up to 2 mm thick.

Keywords:

complex oxides synthesis, magnesium aluminate spinel, optical ceramics

OCIS codes: 160.4236

References:

1. G. P. Val’nin, “Optically transparent ceramic based on yttrium oxide (III) obtained using alkoxy technology,” Author’s Abstract of Dissertation for Candidate, FGUP IREA, Moscow (2008).
2. I. Ganesh, “A review on magnesium aluminate (MgAl2 O4 ) spinel: synthesis, processing and applications,” Int. Mater. Rev. 58, No. 2, 63 (2013).
3. A. Goldstein, A. Goldenberg, and M. Hefetz, “Transparent polycrystalline MgAl2 O4 spinel with submicron grains, by low temperature sintering,” J. Ceram. Soc. Jpn. 117, 1281 (2009).
4. S. K. Behera, P. Barpanda, S. K. Pratihar, and S. Bhattacharyya, “Synthesis of magnesium-aluminium spinel from autoignition of citrate–nitrate gel,” Mater. Lett. 58, 1451 (2004).
5. A. S. Maia, R. Stefani, C. A. Kodaira, C. F. C. Felinto, E. E. S. Teotonio, and H. F. Brito, “Luminescent nanoparticles of MgAl2O 4: Eu, Dy prepared by citrates sol–gel method,” Opt. Mater. 31, 440 (2008).
6. L.-Z. Pei, W.-Y. Yin, J.-F. Wang, J. Chen, C.-G. Fan, and Q.-F. Zhang, “Low-temperature synthesis of magnesium oxide and spinel powders by a sol–gel process,” Mater. Res. 13, 339 (2010).
7. W. Liu, D. Wu, and J. Yang, “Preparation of nanometer magnesium aluminate spinel powders by sol–gel method,” Int. J. Mater. Prod. Technol. 37, 297 (2010).
8. V. V. Drobotenko and E. M. Gavrishchuk, “Method of obtaining double magnesium–aluminum isopropylate,” Russian Patent No. 2,471,763 (2011).
9. M. P. Pechini, “Method of preparing lead and alkaline earth titanates and niobates and coating method using the same to form a capacitor,” U.S. Patent 3,330,697, July 11, 1967.
10. E. V. Gol’eva and M. D. Mikhaı˘lov, “Synthesis of nanosize particles of yttrium tungstate in salt melts,” in Science Week of St. Petersburg State Polytechnic University. Best Reports: Materials of the Scientific–Practical Conference with International Participation (Izd. Politekh. Univ., St. Petersburg, 2013), pp. 106–109.
11. D. V. Tolstikova, M. D. Mikhaı˘lov, and V. M. Smirnov, “Synthesis of nanoparticles of magnesium aluminate spinel in a melt of potassium chloride,” in Collected Transactions of the Conference on Future Optics (S. I. Vavilov State Optical Institute, 2013), pp. 76–78.
12. V. D. Andreeva, Special Methods of X-ray Diffraction and Electron-Microscopic Studies of Materials (Izd. Politekh. Univ., St. Petersburg, 2008).